Search results for "Glassy carbon electrode"

showing 2 items of 2 documents

A glassy carbon electrode modified by a triply-fused-like Co( ii ) polyporphine and its ability for sulphite oxidation and detection

2018

This article presents a Co(II) polyporphine conductive polymer easily and rapidly obtained (less than 2 h 30 min) on the surface of a glassy carbon electrode from the transformation of an initial Mg(II) porphine solution in a four-step process (including electrochemical and chemical stages). The intimate molecular structure is argued on the basis of the electrochemical response of the modified electrode, as well as its surface characterization. Owing to its apparent stability in water over potential cycling and its high density in active Co(II) centers, the electrosynthesized film shows its ability to catalyze sulphite oxidation in aqueous solutions. The mechanism of this molecular catalysi…

Conductive polymerDetection limitAqueous solutionChemistry[CHIM.ORGA]Chemical Sciences/Organic chemistryGlassy carbon electrodeInorganic chemistry02 engineering and technologyGeneral Chemistry[CHIM.MATE]Chemical Sciences/Material chemistry010402 general chemistry021001 nanoscience & nanotechnologyElectrochemistry01 natural sciencesCatalysis0104 chemical sciencesCatalysis[CHIM.ANAL]Chemical Sciences/Analytical chemistryElectrodeMaterials ChemistryMolecule[CHIM.COOR]Chemical Sciences/Coordination chemistry0210 nano-technology
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Discrimination of papers used in conservation and restoration by the means of the voltammetry of immobilized microparticles technique

2019

Herein, voltammetry of immobilized microparticles (VIMP) is employed for the discrimination of papers used in the conservation and restoration field. The electrochemical parameters are used for the discrimination of different samples coming from China, Japan and Korea. The method is based on the recording of the voltammetric response of microparticulate deposits from acetone extracts of paper samples deposited on a glassy carbon electrode in contact with 1.0 M H2SO4. The voltammetric responses attributed to the lignin and the oxidation products of the cellulose were collected and are discussed. The grouping of samples was obtained upon the application of the chemometric methods, as well as …

Materials scienceGeneral Chemical Engineering010401 analytical chemistryGlassy carbon electrodeGeneral EngineeringAnalytical chemistry02 engineering and technology021001 nanoscience & nanotechnology01 natural sciences0104 chemical sciencesAnalytical ChemistryChemometricsConservationManufacturing methods0210 nano-technologyVoltammetryAnalytical Methods
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